D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Base Information

Chemical Name:D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate
CAS No.:438035-30-4
Molecular Formula:C₃₀H₃₂O₇
Molecular Weight:504.58
Hs Code.:

Synonyms:D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Suppliers and Price of D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

There total 5 articles about D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 65-85-0,8013-63-6
benzoic acid

: 219562-56-8,173828-64-3
D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-myo-inositol

: 438035-30-4
D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 80 ℃;
DOI:10.1016/S0960-894X(03)00629-2

Reference yield:

: 266682-75-1
(3aR,4S,7S,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-di-O-benzyl-2,3-benzodioxole-4,7-diol

: 438035-30-4
D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 94.4 percent / OsO₄; NMO / acetone; H₂O

2: 79 percent / Ph₃P; DEAD / toluene / 80 °C

With osmium(VIII) oxide; N-methyl-2-indolinone; triphenylphosphine; diethylazodicarboxylate; In water; acetone; toluene; 2: Mitsunobu reaction;
DOI:10.1016/S0960-894X(03)00629-2

Reference yield:

: 371155-65-6
(3aR,4S,7S,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-1,3-benzodioxole-4,7-diol

: 438035-30-4
D-4,5-O-(1-methylethylidene)-3,6-bis-O-(phenylmethyl)-scyllo-inositol 1-monobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / NaH / dimethylformamide

2: 94.4 percent / OsO₄; NMO / acetone; H₂O

3: 79 percent / Ph₃P; DEAD / toluene / 80 °C

With osmium(VIII) oxide; N-methyl-2-indolinone; sodium hydride; triphenylphosphine; diethylazodicarboxylate; In water; N,N-dimethyl-formamide; acetone; toluene; 3: Mitsunobu reaction;
DOI:10.1016/S0960-894X(03)00629-2