(E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

Base Information

Chemical Name:(E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone
CAS No.:117607-08-6
Molecular Formula:C₁₆H₁₄N₄O
Molecular Weight:278.313
Hs Code.:

Synonyms:(E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

Suppliers and Price of (E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

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Technology Process of (E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

There total 4 articles about (E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 98326-49-9
(E)-4,5-dihydro-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3(2H)-pyridazinone

: 117607-08-6
(E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

Guidance literature:: With manganese(IV) oxide; In tetrahydrofuran; for 18h; Heating;
DOI:10.1021/jm00122a011

Reference yield:

: 6628-79-1
3-methyllevulinic acid

: 117607-08-6
(E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / piperidine / toluene / 6 h / Heating

2: 44 percent / hydrazine hydrate, glacial acetic acid / 30 h / Heating

3: 15 percent / MnO₂ / tetrahydrofuran / 18 h / Heating

With piperidine; manganese(IV) oxide; hydrazine hydrate; acetic acid; In tetrahydrofuran; toluene;
DOI:10.1021/jm00122a011

Reference yield:

: 10040-98-9
1-(4-formylphenyl)-1H-imidazole

: 117607-08-6
(E)-6-<2-<4-(1H-imidazol-1-yl)phenyl>ethenyl>-5-methyl-3-(2H)-pyridazinone

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / piperidine / toluene / 6 h / Heating

2: 44 percent / hydrazine hydrate, glacial acetic acid / 30 h / Heating

3: 15 percent / MnO₂ / tetrahydrofuran / 18 h / Heating

With piperidine; manganese(IV) oxide; hydrazine hydrate; acetic acid; In tetrahydrofuran; toluene;
DOI:10.1021/jm00122a011