Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

Base Information

Chemical Name:Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester
CAS No.:870862-63-8
Molecular Formula:C₃₅H₆₂NO₆P
Molecular Weight:623.854
Hs Code.:

Synonyms:Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

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Chemical Property of Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

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Technology Process of Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

There total 8 articles about Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 851589-01-0
phosphoric acid di-tert-butyl ester 3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-octadec-9-enoylamino-propyl ester

: 870862-63-8
Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

Guidance literature:: tetrabutyl ammonium fluoride; In tetrahydrofuran;

Reference yield:

: 3728-20-9
D-tyrosine methylester hydrochloride

: 870862-63-8
Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: DIEA / CH₂Cl₂ / 4 h

2: DIEA; DMAP / 2 h

3: NaBH₄; CaCl₂ / ethanol; tetrahydrofuran / 18 h

4: tetrazole / 4 h

5: aq. H₂O₂ / 4 h

6: TBAF*3H₂O / tetrahydrofuran / 1 h

With 1H-tetrazole; dmap; sodium tetrahydroborate; tetrabutyl ammonium fluoride; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; calcium chloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2004.05.023

Reference yield:

: 851588-99-3
(R)-3-[4-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-2-((Z)-octadec-9-enoylamino)-propionic acid methyl ester

: 870862-63-8
Phosphoric acid di-tert-butyl ester (R)-3-(4-hydroxy-phenyl)-2-((Z)-octadec-9-enoylamino)-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄; CaCl₂ / ethanol; tetrahydrofuran / 18 h

2: tetrazole / 4 h

3: aq. H₂O₂ / 4 h

4: TBAF*3H₂O / tetrahydrofuran / 1 h

With 1H-tetrazole; sodium tetrahydroborate; tetrabutyl ammonium fluoride; dihydrogen peroxide; calcium chloride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2004.05.023