2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester

Base Information

• Chemical Name: 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester
• CAS No.: 866483-14-9
• Molecular Formula: C₂₈H₂₉NO₄Se
• Molecular Weight: 522.503

Synonyms:2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester

Chemical Property of 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester

Chemical Property:

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Technology Process of 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester

There total 5 articles about 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

9-Fluorenylmethanol (24324-17-2) + (S)-2-tert-butoxycarbonylamino-3-phenylselanylpropionic acid (179087-83-3) → 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester (866483-14-9)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃;

DOI:10.1073/pnas.2021847118

Reference yield:

Benzeneselenol (645-96-5) → 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester (866483-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide / 2 h / 20 °C

2: 1,3-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 4 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2005.07.122

Reference yield:

(S)-3-(tert-butoxycarbonylamino)-oxetan-2-one (98541-64-1) → 2-tert-butoxycarbonylamino-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester (866483-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide / 2 h / 20 °C

2: 1,3-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 4 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2005.07.122

upstream raw materials:

9-Fluorenylmethanol

(S)-2-tert-butoxycarbonylamino-3-phenylselanylpropionic acid

(S)-3-(tert-butoxycarbonylamino)-oxetan-2-one

Benzeneselenol

Downstream raw materials:

2-(2-tert-butoxycarbonylamino-3-phenylselanyl-propionylamino)-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester

(R)-2-((R)-2-Amino-3-phenylselanyl-propionylamino)-3-phenylselanyl-propionic acid 9H-fluoren-9-ylmethyl ester

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