allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

Base Information

Chemical Name:allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside
CAS No.:1443672-56-7
Molecular Formula:C₅₇H₆₂O₁₁
Molecular Weight:923.113
Hs Code.:

Synonyms:allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

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Chemical Property of allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

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Technology Process of allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

There total 1 articles about allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1443672-55-6
allyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-4,6-benzylidene-β-D-mannopyranosyl)-α-D-mannopyranoside

: 1443672-56-7
allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 7h;
DOI:10.1021/jo4005266

Reference yield: 61.0%

: 1443672-56-7
allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

: 159407-17-7
phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 1443672-83-0
allyl 2,3-di-O-benzyl-4,6-benzylidene-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside; With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.0833333h; Molecular sieve; Inert atmosphere;

allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside; In dichloromethane; at -78 - 20 ℃; stereoselective reaction;
DOI:10.1021/jo4005266

Reference yield: 53.0%

: 1443672-56-7
allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside

: 159353-70-5
phenyl 2-O-p-methoxybenzyl-3-O-benzyl-4,6-O-benzylidene-1-deoxy-1-thio-α-D-mannopyranoside

: allyl 3-O-benzyl-4,6-benzylidene-2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: phenyl 2-O-p-methoxybenzyl-3-O-benzyl-4,6-O-benzylidene-1-deoxy-1-thio-α-D-mannopyranoside; With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.0833333h; Molecular sieve; Inert atmosphere;

allyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-trii-O-benzyl-β-D-mannopyranosyl)-α-D-mannopyranoside; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo4005266