N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

Base Information

Chemical Name:N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide
CAS No.:1310048-44-2
Molecular Formula:C₁₉H₂₃N₅O₄
Molecular Weight:385.423
Hs Code.:

Synonyms:N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

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Technology Process of N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

There total 5 articles about N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1310048-43-1
4-(aminomethyl)-N-(3-azidopropyl)benzamide

: 95298-68-3
3-methoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

: 1310048-44-2
N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 45 ℃; Inert atmosphere;
DOI:10.1002/anie.201007871

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 1310048-44-2
N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 20 °C / Inert atmosphere

2: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

3: triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4: ethanolamine / dichloromethane / 3 h / Inert atmosphere

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 45 °C / Inert atmosphere

With dmap; sodium hydrogencarbonate; ethanolamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201007871

Reference yield:

: 503470-09-5
C₂₉H₁₈F₅NO₄

: 1310048-44-2
N-(3-azidopropyl)-4-((3-methoxy-5-oxocyclohex-3-enecarboxamido)methyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: ethanolamine / dichloromethane / 3 h / Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 45 °C / Inert atmosphere

With dmap; ethanolamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201007871