C₂₉H₃₂N₆Si

Base Information

Chemical Name:C₂₉H₃₂N₆Si
CAS No.:1334313-80-2
Molecular Formula:C₂₉H₃₂N₆Si
Molecular Weight:492.699
Hs Code.:

C<sub>29</sub>H<sub>32</sub>N<sub>6</sub>Si

Synonyms:C₂₉H₃₂N₆Si

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Chemical Property of C₂₉H₃₂N₆Si

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Technology Process of C₂₉H₃₂N₆Si

There total 16 articles about C₂₉H₃₂N₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334313-79-9
C₃₉H₄₈N₆O₄Si

: 1334313-80-2
C₂₉H₃₂N₆Si

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 268224-27-7
(R)-1-tert-butyl-5-methyl 3,3-dimethyl-1,3-azasilolidine-1,5-dicarboxylate

: 1334313-80-2
C₂₉H₃₂N₆Si

Guidance literature:: Multi-step reaction with 5 steps

1: water; potassium hydroxide / methanol / 15 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C

3: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 120 °C

4: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 15 h / Inert atmosphere; Reflux

5: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium acetate; water; sodium carbonate; triethylamine; trifluoroacetic acid; potassium hydroxide; In 1,4-dioxane; methanol; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 268224-29-9
(R)-3,3-dimethyl-[1,3]azasilolidine-1,5-dicarboxylic acid 1-tert-butyl ester

: 1334313-80-2
C₂₉H₃₂N₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C

2: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 120 °C

3: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 15 h / Inert atmosphere; Reflux

4: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium acetate; sodium carbonate; triethylamine; trifluoroacetic acid; In 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; N,N-dimethyl-formamide;