3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

Base Information

Chemical Name:3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid
CAS No.:913987-17-4
Molecular Formula:C₂₇H₃₄N₂O₆
Molecular Weight:482.577
Hs Code.:

Synonyms:3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

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Chemical Property of 3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

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Technology Process of 3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

There total 3 articles about 3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 913987-17-4
3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 13.8 g / EDC; DIEA / dimethylformamide

2: 85 percent / DIEA / dimethylformamide

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1039/b609446e

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 913987-17-4
3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaOH / dioxane; H₂O / 0 - 20 °C

2: 13.8 g / EDC; DIEA / dimethylformamide

3: 85 percent / DIEA / dimethylformamide

With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1039/b609446e

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 913987-17-4
3-(4-benzoylphenyl)-2-(6-(tert-butoxycarbonyl)hexanamido)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaOH / dioxane; H₂O / 0 - 20 °C

2: 13.8 g / EDC; DIEA / dimethylformamide

3: 85 percent / DIEA / dimethylformamide

With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1039/b609446e