2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Base Information

Chemical Name:2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate
CAS No.:1448318-96-4
Molecular Formula:C₁₄H₁₉F₅O₅S
Molecular Weight:394.36
Hs Code.:

2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ<sup>6</sup>-sulphanyl)benzoate

Synonyms:2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

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Chemical Property of 2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

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Technology Process of 2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

There total 4 articles about 2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1448317-72-3
3-(hydroxymethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoic acid

: 6482-24-2
2-Bromoethyl methyl ether

: 1448318-96-4
2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

: 1448318-97-5
2-methoxyethyl 3-(hydroxymethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Guidance literature:: 3-(hydroxymethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoic acid; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;

2-Bromoethyl methyl ether; In N,N-dimethyl-formamide; mineral oil; at 60 ℃; for 16h;

Reference yield:

: 833-96-5
3-(pentafluoro-λ⁶-sulphanyl)benzoic acid

: 1448318-96-4
2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; trifluoroacetic acid; N-Bromosuccinimide / 18 h / 50 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 0.5 h / Cooling with ice

2.2: 0.5 h / Cooling with ice

3.1: sodium tris(acetoxy)borohydride; acetic acid; azetion-3-ol hydrochloride / dichloromethane / 1 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

4.2: 16 h / 60 °C

With N-Bromosuccinimide; sulfuric acid; azetion-3-ol hydrochloride; isopropylmagnesium chloride; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1180675-98-2
3-bromo-5-(pentafluoro-λ⁶-sulphanyl)benzoic acid

: 1448318-96-4
2-methoxyethyl 3-[(2-methoxyethoxy)methyl]-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 0.5 h / Cooling with ice

1.2: 0.5 h / Cooling with ice

2.1: sodium tris(acetoxy)borohydride; acetic acid; azetion-3-ol hydrochloride / dichloromethane / 1 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

3.2: 16 h / 60 °C

With azetion-3-ol hydrochloride; isopropylmagnesium chloride; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; mineral oil;