2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester

Base Information

• Chemical Name: 2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester
• CAS No.: 1481751-14-7
• Molecular Formula: C₂₀H₂₁NO₃
• Molecular Weight: 323.392
• Mol file: 1481751-14-7.mol

Synonyms:2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester

Chemical Property of 2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester

There total 1 articles about 2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-o-xylene (95-64-7) → 2,3,7-trimethyl-9-oxo-10(9H)-acridineacetic acid ethyl ester (1481751-14-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate; copper / pentan-1-ol / 3 h / Reflux

2.1: trichlorophosphate / acetonitrile / 3 h / Reflux

2.2: 0.5 h / 20 °C

2.3: 24 h / 0 - 20 °C

With copper; potassium carbonate; trichlorophosphate; In pentan-1-ol; acetonitrile; 1.1: |Ullmann Condensation;

DOI:10.1021/jo401683r

upstream raw materials:

4-amino-o-xylene