diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

Base Information

Chemical Name:diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate
CAS No.:852947-18-3
Molecular Formula:C₂₃H₃₂NO₆P
Molecular Weight:449.484
Hs Code.:

Synonyms:diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

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Chemical Property of diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

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Technology Process of diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

There total 2 articles about diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

: C₁₉H₂₁NO₃

: 852947-18-3
diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

Guidance literature:: triethylamine; In hexanes; for 3h; Heating / reflux;

Reference yield:

: C₂₀H₂₂Cl₃NO₄

: 762-04-9
phosphonic acid diethyl ester

: 852947-18-3
diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

Guidance literature:: With triethylamine; In hexane; at 20 - 80 ℃; Inert atmosphere;
DOI:10.1021/jm800824d

Reference yield: 42.0%

: 852947-18-3
diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate

: 852947-17-2
N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonic acid

Guidance literature:: diethyl N-[3,5-dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)]carbamonylphosphonate; With trimethylsilyl bromide; In dichloromethane; at -78 - 20 ℃; for 16h;

With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 16h;

With water; In dichloromethane; at 0 ℃;