ethyl 6-bromo-4-hydroxy-5-methoxy-2-methyl-1-(4-methylphenyl)-7-(2-oxopropyl)-1H-indole-3-carboxylate

Base Information

Chemical Name:ethyl 6-bromo-4-hydroxy-5-methoxy-2-methyl-1-(4-methylphenyl)-7-(2-oxopropyl)-1H-indole-3-carboxylate
CAS No.:114261-87-9
Molecular Formula:C₂₃H₂₄BrNO₅
Molecular Weight:474.351
Hs Code.:
Mol file:114261-87-9.mol

Synonyms:1-(p-tolyl)-2-methyl-3-ethoxycarbonyl-4-hydroxy-5-methoxy-6-bromo-7-acetonylindole

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Chemical Property of ethyl 6-bromo-4-hydroxy-5-methoxy-2-methyl-1-(4-methylphenyl)-7-(2-oxopropyl)-1H-indole-3-carboxylate

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Technology Process of ethyl 6-bromo-4-hydroxy-5-methoxy-2-methyl-1-(4-methylphenyl)-7-(2-oxopropyl)-1H-indole-3-carboxylate

There total 2 articles about ethyl 6-bromo-4-hydroxy-5-methoxy-2-methyl-1-(4-methylphenyl)-7-(2-oxopropyl)-1H-indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 77-78-1
dimethyl sulfate

: 114261-85-7
6-Bromo-4,5-dihydroxy-2-methyl-7-(2-oxo-propyl)-1-p-tolyl-1H-indole-3-carboxylic acid ethyl ester

: 114261-87-9
1-(p-tolyl)-2-methyl-3-ethoxycarbonyl-4-hydroxy-5-methoxy-6-bromo-7-acetonylindole

Guidance literature:: With potassium carbonate; In acetone; for 7h; Heating;
DOI:10.1007/BF00473453

Reference yield:

: 84716-34-7
6-Bromo-7-(1-ethoxycarbonyl-2-oxo-propyl)-4,5-dihydroxy-2-methyl-1-p-tolyl-1H-indole-3-carboxylic acid ethyl ester

: 114261-87-9
1-(p-tolyl)-2-methyl-3-ethoxycarbonyl-4-hydroxy-5-methoxy-6-bromo-7-acetonylindole

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / orthophosphoric acid / acetic acid / 12 h / Heating

2: 84 percent / anhydrous potassium carbonate / acetone / 7 h / Heating

With phosphoric acid; potassium carbonate; In acetic acid; acetone;
DOI:10.1007/BF00473453