(1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine

Base Information

• Chemical Name: (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine
• CAS No.: 93128-50-8
• Molecular Formula: C₂₀H₃₀N₂
• Molecular Weight: 298.472

Synonyms:(1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine

Chemical Property of (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine

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Technology Process of (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine

There total 3 articles about (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

α,α,α',α'-tetramethyldipropargylamine (2809-93-0) + ethyl cinnamate (4192-77-2) → (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine (93128-50-8) + Methyl 1,1,3,3-tetramethyl-6-phenyl-2,3,5α,6β-tetrahydro-1H-isoindole-5-carboxylate

Guidance literature:

With bis(acetonitrile)bis(diethyl fumarate)cobalt⁽⁰⁾; In toluene; at 80 ℃; for 5h;

Reference yield:

α,α,α',α'-tetramethyldipropargylamine (2809-93-0) + phenylacetylene (536-74-3) → (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine (93128-50-8) + Tetramethyl-5-phenyl-2,3-dihydro-1,1,3,3-1H-isoindole (86762-52-9)

Guidance literature:

With bis(acetonitrile)bis(diethyl fumarate)cobalt⁽⁰⁾; In acetonitrile; at 80 ℃; for 72h;

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + α,α,α',α'-tetramethyldipropargylamine (2809-93-0) → (1,1-Dimethyl-prop-2-ynyl)-[1-methyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-5-yl)-ethyl]-amine (93128-50-8) + 1,1,3,3-Tetramethyl-5-phenyl-2,3,5,6-tetrahydro-1H-isoindole (142836-91-7)

Guidance literature:

With dicobalt octacarbonyl; In toluene; at 80 ℃; for 7h;

upstream raw materials:

styrene

α,α,α',α'-tetramethyldipropargylamine

phenylacetylene

ethyl cinnamate

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