C₂₈H₁₈BrN

Base Information

Chemical Name:C₂₈H₁₈BrN
CAS No.:1210470-10-2
Molecular Formula:C₂₈H₁₈BrN
Molecular Weight:448.362
Hs Code.:

Synonyms:C₂₈H₁₈BrN

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Chemical Property of C₂₈H₁₈BrN

Chemical Property:

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Technology Process of C₂₈H₁₈BrN

There total 8 articles about C₂₈H₁₈BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1210470-04-4
C₂₈H₁₉N

: 1210470-10-2
C₂₈H₁₈BrN

Guidance literature:: With N-Bromosuccinimide; In chloroform; for 5h;

Reference yield:

: 59-88-1
phenylhydrazine hydrochloride

: 1210470-10-2
C₂₈H₁₈BrN

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid / ethanol / 2 h / Reflux; Inert atmosphere

2: chloranil / xylene / 2 h / Inert atmosphere; Reflux

3: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / xylene / 5 h / Inert atmosphere; Reflux

4: pyridine hydrochloride / 0.67 h / Heating

5: pyridine / dichloromethane / 0 °C

6: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 3 h / Reflux

7: N-Bromosuccinimide / chloroform / 5 h

With pyridine; N-Bromosuccinimide; pyridine hydrochloride; chloranil; potassium carbonate; acetic acid; sodium t-butanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; xylene; 6: Suzuki Coupling;

Reference yield:

: 1210469-95-6
C₂₃H₁₇NO

: 1210470-10-2
C₂₈H₁₈BrN

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine hydrochloride / 0.67 h / Heating

2: pyridine / dichloromethane / 0 °C

3: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 3 h / Reflux

4: N-Bromosuccinimide / chloroform / 5 h

With pyridine; N-Bromosuccinimide; pyridine hydrochloride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; chloroform; water; 3: Suzuki Coupling;