[3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

Base Information

Chemical Name:[3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester
CAS No.:366784-90-9
Molecular Formula:C₁₆H₂₂NO₅P
Molecular Weight:339.328
Hs Code.:

Synonyms:[3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

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Chemical Property of [3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

Chemical Property:

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Technology Process of [3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

There total 4 articles about [3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 366784-84-1
2-benzoyl-5-(diethoxy-phosphoryl)-pentanoic acid ethyl ester

: 366784-90-9
[3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; Heating;
DOI:10.1039/b101751i

Reference yield:

: 1067-87-4
Diethyl allylphosphonate

: 366784-90-9
[3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 85 percent / Bu₃SnH; AIBN / cyclohexane / Heating

3: 74 percent / NH₂OH*HCl; AcONa / ethanol / Heating

With 2,2'-azobis(isobutyronitrile); dilauryl peroxide; hydroxylamine hydrochloride; tri-n-butyl-tin hydride; sodium acetate; In ethanol; cyclohexane; 1,2-dichloro-ethane;
DOI:10.1039/b101751i

Reference yield:

: 2-ethoxythiocarbonylsulfanyl-3-oxo-3-phenyl-propionic acid ethyl ester

: 366784-90-9
[3-(5-oxo-3-phenyl-4,5-dihydro-isoxazol-4-yl)-propyl]-phosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 85 percent / Bu₃SnH; AIBN / cyclohexane / Heating

3: 74 percent / NH₂OH*HCl; AcONa / ethanol / Heating

With 2,2'-azobis(isobutyronitrile); dilauryl peroxide; hydroxylamine hydrochloride; tri-n-butyl-tin hydride; sodium acetate; In ethanol; cyclohexane; 1,2-dichloro-ethane;
DOI:10.1039/b101751i