Technology Process of (3aS,4S,6S,7aR)-2-(3-ethylbenzyl)-3a,5,5-trimethylhexahydro-4,6-methanobenzo[d][1,3,2]dioxaborole
There total 5 articles about (3aS,4S,6S,7aR)-2-(3-ethylbenzyl)-3a,5,5-trimethylhexahydro-4,6-methanobenzo[d][1,3,2]dioxaborole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
diethyl ether;
at 20 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 12 h / 100 °C
2: diethyl ether / 12 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; diethyl ether;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus tribromide / diethyl ether / 0.5 h / 0 °C
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 12 h / 100 °C
3: diethyl ether / 12 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); phosphorus tribromide; potassium carbonate;
In
1,4-dioxane; diethyl ether;
