1-methyl-5-indolethiol

Base Information

Chemical Name:1-methyl-5-indolethiol
CAS No.:101273-62-5
Molecular Formula:C₉H₉NS
Molecular Weight:163.243
Hs Code.:

Synonyms:1-methyl-5-indolethiol

Suppliers and Price of 1-methyl-5-indolethiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
1-methyl-1H-Indole-5-thiol 97.00%
25G
$ 9900.00

AccelPharmtech
1-methyl-1H-Indole-5-thiol 97.00%
5G
$ 5270.00

AccelPharmtech
1-methyl-1H-Indole-5-thiol 97.00%
1G
$ 3060.00

Total 0 raw suppliers

Chemical Property of 1-methyl-5-indolethiol

Chemical Property:

Purity/Quality:: 1-methyl-1H-Indole-5-thiol 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-methyl-5-indolethiol

There total 3 articles about 1-methyl-5-indolethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 280752-86-5
1-methyl-S-triisopropylsilyl-5-indolethiol

: 101273-62-5
1-methyl-5-indolethiol

Guidance literature:: With cesium fluoride; In 1-methyl-pyrrolidin-2-one;
DOI:10.1021/jm0103108

Reference yield:

: 16066-91-4
5-iodo-1H-indole

: 101273-62-5
1-methyl-5-indolethiol

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1 h / -78 °C

1.2: 99 percent / tetrahydrofuran / 16 h / 25 °C

2.1: KH / tetrahydrofuran / 2 h / 5 - 25 °C

2.2: 88 percent / (Ph₃P)4Pd / tetrahydrofuran / 1 h / 70 °C

3.1: CsF / 1-methyl-pyrrolidin-2-one

With potassium hydride; sodium hydride; cesium fluoride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
DOI:10.1021/jm0103108

Reference yield:

: 280563-07-7
1-methyl-5-iodoindole

: 101273-62-5
1-methyl-5-indolethiol

Guidance literature:: Multi-step reaction with 2 steps

1.1: KH / tetrahydrofuran / 2 h / 5 - 25 °C

1.2: 88 percent / (Ph₃P)4Pd / tetrahydrofuran / 1 h / 70 °C

2.1: CsF / 1-methyl-pyrrolidin-2-one

With potassium hydride; cesium fluoride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
DOI:10.1021/jm0103108