N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

Base Information

Chemical Name:N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane
CAS No.:1310361-03-5
Molecular Formula:C₃₁H₃₈N₂O₄Si
Molecular Weight:530.739
Hs Code.:

Synonyms:N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

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Chemical Property of N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

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Technology Process of N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

There total 3 articles about N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1310360-86-1
4-nitrophenyl 2-(triphenylsilyl)ethyl carbonate

: 1310360-98-5
N-alloc-1,6-diaminohexane hydrotrifluoroacetate

: 1310361-03-5
N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.3390/molecules16064695

Reference yield:

: 18666-68-7
vinyltriphenylsilane

: 1310361-03-5
N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

1.2: 3 h / 45 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With pyridine; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules16064695

Reference yield:

: 18666-87-0
1,1,1-triphenyl-1-silapropan-3-ol

: 1310361-03-5
N-(2-(triphenylsilyl)ethoxy)carbonyl-N'-allyloxycarbonyl-1,6-diaminohexane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With pyridine; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules16064695