1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

Base Information

Chemical Name:1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin
CAS No.:1365691-93-5
Molecular Formula:C₅₈H₇₀N₆O₂₂
Molecular Weight:1203.22
Hs Code.:

Synonyms:1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

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Chemical Property of 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

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Technology Process of 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

There total 1 articles about 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 40371-50-4
S-4-benzyloxycarbonylamino-2-hydroxybutyric acid

: 1365691-91-3
1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-apramycin

: 1365691-93-5
1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

Guidance literature:: S-4-benzyloxycarbonylamino-2-hydroxybutyric acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 26 ℃; for 2h;

1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-apramycin; With triethylamine; In tetrahydrofuran; for 20h;

Reference yield: 85.0%

: 1365691-93-5
1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

: 7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxybutyryl]apramycin tetraacetate

Guidance literature:: With 20% palladium hydroxide-activated charcoal; hydrogen; acetic acid; In 1,4-dioxane; water; for 15h; under 760.051 Torr;

Reference yield: 12.0%

: 1365691-93-5
1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin

: 1365691-94-6
4-N-[(2S)-4-amino-2-hydroxybutyryl]apramycin

Guidance literature:: 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4"-N-[(2S)-4-amino-2-hydroxy-butyryl]apramycin; With barium hydroxide monohydrate; In 1,4-dioxane; water; at 50 ℃; for 6h;

With 20% palladium hydroxide-activated charcoal; hydrogen; acetic acid; In water; for 15h; under 760.051 Torr;