(2R,3R,11bS)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine-2-ethanol

Base Information

• Chemical Name: (2R,3R,11bS)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzo
• Molecular Formula: C₂₅H₃₃NO₃
• Molecular Weight: 395.542

Synonyms:(2R,3R,11bS)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine-2-ethanol

Chemical Property of (2R,3R,11bS)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzo

Chemical Property:

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There total 2 articles about (2R,3R,11bS)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine-2-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(2R,3R,11bS)-(-)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine-2-acetic acid ethyl ester (82310-54-1) → (2R,3R,11bS)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine-2-ethanol (84922-66-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Ambient temperature;

Reference yield: 91.0%

(+/-)-10-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine-2β-acetic acid ethyl ester (73053-58-4,82310-54-1) → (+/-)-10-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine-2β-ethanol (84922-66-7,84985-53-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; 1.) room temp., 1 h; 2.) reflux, 10 min;

upstream raw materials:

(+/-)-10-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine-2β-acetic acid ethyl ester

(2R,3R,11bS)-(-)-10-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine-2-acetic acid ethyl ester

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