Technology Process of benzyl 5-O-benzoyl-β-D-ribofuranoside
There total 1 articles about benzyl 5-O-benzoyl-β-D-ribofuranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) dibutyltin oxide / 1.) toluene, reflux, 3 h, 2.) N,N-dimethylformamide, 48 h, 70 deg C
2: 81 percent / silver triflate, Drierite / CH2Cl2 / 0.17 h / -25 °C
3: 65 percent / hydrogen, palladium oxide / methanol; ethyl acetate / Ambient temperature
With
palladium(II) oxide; calcium sulfate; hydrogen; silver trifluoromethanesulfonate; di(n-butyl)tin oxide;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1016/0008-6215(84)85223-4
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) dibutyltin oxide / 1.) toluene, reflux, 3 h, 2.) N,N-dimethylformamide, 48 h, 70 deg C
2: 81 percent / silver triflate, Drierite / CH2Cl2 / 0.17 h / -25 °C
3: 65 percent / hydrogen, palladium oxide / methanol; ethyl acetate / Ambient temperature
4: 97 percent / pyridine / 3 h / Ambient temperature
5: 162 mg / TiBr4 / CH2Cl2 / 18 h / 4 °C
6: 43 percent / silver triflate, Drierite / CH2Cl2 / 0.33 h / -15 °C
With
pyridine; palladium(II) oxide; calcium sulfate; hydrogen; silver trifluoromethanesulfonate; titanium(IV) bromide; di(n-butyl)tin oxide;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1016/0008-6215(84)85223-4
