(5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

Base Information

Chemical Name:(5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane
CAS No.:851636-85-6
Molecular Formula:C₂₀H₃₁BrOSi
Molecular Weight:395.455
Hs Code.:

Synonyms:(5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

Suppliers and Price of (5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

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Technology Process of (5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

There total 2 articles about (5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17211-08-4
(4-bromo-benzyl)-phosphonic acid dimethyl ester

: 422511-04-4
(E)-7-(tert-butyldimethylsilanyloxy)hept-2-enal

: 851636-85-6
(5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1021/ja050214m

Reference yield:

: 589-15-1
1-bromomethyl-4-bromobenzene

: 851636-85-6
(5E,7E)-8-((4'-bromophenyl)octa-5,7-dienyloxyl)-(tert-butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 20 h / 150 °C

2: 84 percent / t-BuOK / tetrahydrofuran / 1 h / 0 - 20 °C

With potassium tert-butylate; In tetrahydrofuran; 1: Arbuzov reaction;
DOI:10.1021/ja050214m