Technology Process of tert-butyl 4-<(6-aminoindazol-1-yl)methyl>-3-methoxybenzoate
There total 6 articles about tert-butyl 4-<(6-aminoindazol-1-yl)methyl>-3-methoxybenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; acetic acid; ethyl acetate;
palladium on activated charcoal;
for 24h;
under 2585.7 Torr;
DOI:10.1021/jm00168a036
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / K2CO3 / acetone / 48 h / Heating
2: 100 percent / acetic acid-EtOAc, H2 / 10percent Pd/C / 24 h / 2585.7 Torr
With
hydrogen; potassium carbonate; acetic acid; ethyl acetate;
palladium on activated charcoal;
In
acetone;
DOI:10.1021/jm00168a036
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 70 percent / conc. H2SO4 / CH2Cl2 / 16 h
2: 95 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 1 h / Heating; Irradiation
3: 98 percent / K2CO3 / acetone / 48 h / Heating
4: 100 percent / acetic acid-EtOAc, H2 / 10percent Pd/C / 24 h / 2585.7 Torr
With
N-Bromosuccinimide; Perbenzoic acid; sulfuric acid; hydrogen; potassium carbonate; acetic acid; ethyl acetate;
palladium on activated charcoal;
In
tetrachloromethane; dichloromethane; acetone;
DOI:10.1021/jm00168a036
