Technology Process of C29H33N6O15PS2
There total 5 articles about C29H33N6O15PS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyrrole; trifluoroacetic acid;
In
dichloromethane;
for 0.0333333h;
Ambient temperature;
DOI:10.1016/S0040-4039(00)88796-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2.) Et3N, H2S / 1.) tetrahydrofuran, -35 deg C, 20 min, 2.) RT, 30 min
2: S8, pyridine / 1 h / Ambient temperature
3: 2,6-lutidine / acetonitrile / 5 h
4: 96 percent / CF3CO2H, pyrrole / CH2Cl2 / 0.03 h / Ambient temperature
With
pyridine; 2,6-dimethylpyridine; sulfur; pyrrole; hydrogen sulfide; triethylamine; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)88796-1
- Guidance literature:
-
Multi-step reaction with 3 steps
1: S8, pyridine / 1 h / Ambient temperature
2: 2,6-lutidine / acetonitrile / 5 h
3: 96 percent / CF3CO2H, pyrrole / CH2Cl2 / 0.03 h / Ambient temperature
With
pyridine; 2,6-dimethylpyridine; sulfur; pyrrole; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)88796-1