Technology Process of C30H20OS2
There total 5 articles about C30H20OS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
2: 96 percent / bis-triphenylphosphinenickel dicarbonyl / bis-(2-methoxy-ethyl) ether / 16 h / Heating
3: 1) t-butylhydroperoxide, cuprous bromide; 2) lithium aluminum hydride
4: 95 percent / pyridinium chlorochromate
5: 86 percent / sodium hydride / tetrahydrofuran / -78 - 0 °C
With
tert.-butylhydroperoxide; lithium aluminium tetrahydride; sodium hydride; bis(triphenylphosphine)nickel(0) dicarbonyl; pyridinium chlorochromate; copper(I) bromide;
In
tetrahydrofuran; diethylene glycol dimethyl ether;
DOI:10.1016/S0040-4039(00)87223-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / pyridinium chlorochromate
2: 86 percent / sodium hydride / tetrahydrofuran / -78 - 0 °C
With
sodium hydride; pyridinium chlorochromate;
In
tetrahydrofuran;
DOI:10.1016/S0040-4039(00)87223-8