2,4,6-tri-(tert-butyl)thiobenzaldehyde

Base Information

• Chemical Name: 2,4,6-tri-(tert-butyl)thiobenzaldehyde
• CAS No.: 84543-57-7
• Molecular Formula: C₁₉H₃₀S
• Molecular Weight: 290.513
• Mol file: 84543-57-7.mol

Synonyms:2,4,6-tri-(tert-butyl)thiobenzaldehyde

Chemical Property of 2,4,6-tri-(tert-butyl)thiobenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6-tri-(tert-butyl)thiobenzaldehyde

There total 2 articles about 2,4,6-tri-(tert-butyl)thiobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

ethyl thioformate (29392-46-9) + 2,4,6-tri-tert-butylphenyllithium (35383-91-6) → 2,4,6-tri-(tert-butyl)thiobenzaldehyde (84543-57-7)

Guidance literature:

DOI:10.1039/c39820001187

Reference yield: 40.0%

2,4,6-tri-t-butylbenzaldehyde hydrazone → 2,4,6-tri-(tert-butyl)thiobenzaldehyde (84543-57-7)

Guidance literature:

With disulfur dichloride; triethylamine;

DOI:10.1039/c39820001187

Reference yield: 100.0%

2,4,6-tri-(tert-butyl)thiobenzaldehyde (84543-57-7) → (2,4,6-tri-tert-butylphenyl)methanethiol (125496-17-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/ja00164a011

upstream raw materials:

ethyl thioformate

2,4,6-tri-tert-butylphenyllithium

Downstream raw materials:

1-(2,4,6-Tri-tert-butyl-phenyl)-ethanethiol

6,8-di-tert-butyl-3,4-dihydro-4,4-dimethyl-1H-2-benzothiine

C₄₆H₇₈S₂

(3S,4S)-3-Methoxy-2-methylene-4-(2,4,6-tri-tert-butyl-phenyl)-thietane