2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Base Information

Chemical Name:2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid
CAS No.:672938-01-1
Molecular Formula:C₁₇H₁₁Cl₂NO₅
Molecular Weight:380.184
Hs Code.:

Synonyms:2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Suppliers and Price of 2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

There total 6 articles about 2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.3%

: 672937-99-4
2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutyronitrile

: 672938-01-1
2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Guidance literature:: With sulfuric acid; In water; N,N-dimethyl-formamide; for 4.5h; Heating;
DOI:10.1002/ardp.200300778

Reference yield:

: 21312-94-7
2-acetylamino-6-acetyl-4-chlorophenol

: 672938-01-1
2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 62.8 percent / pyridine / 0 - 100 °C

2: 96.4 percent / NaOH / H₂O; ethanol / 8 h / 20 °C

3: 98.33 percent / glycerin / methanol / 2.5 h / Heating

4: 51.3 percent / H₂SO₄ / H₂O; dimethylformamide / 4.5 h / Heating

With sodium hydroxide; sulfuric acid; glycerol; In pyridine; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ardp.200300778

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 672938-01-1
2-(2-chlorophenyl)-4-(5-chloro-2-oxo-3H-benzoxazol-7-yl)-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 96.4 percent / NaOH / H₂O; ethanol / 8 h / 20 °C

2: 98.33 percent / glycerin / methanol / 2.5 h / Heating

3: 51.3 percent / H₂SO₄ / H₂O; dimethylformamide / 4.5 h / Heating

With sodium hydroxide; sulfuric acid; glycerol; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ardp.200300778