1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

Base Information

Chemical Name:1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole
CAS No.:917247-59-7
Molecular Formula:C₂₇H₂₇Cl₂NO₆S
Molecular Weight:564.486
Hs Code.:

Synonyms:1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

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Chemical Property of 1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

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Technology Process of 1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

There total 3 articles about 1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 917247-56-4
2-benzylthio-5,6-dichloro-3-(2,3-O-isopropylidene-β-D-ribofuranosyl)indole

: 108-24-7
acetic anhydride

: 917247-59-7
1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1080/15257770500265646

Reference yield:

: sodium; 5,6-dichloro-3-(6-hydroxymethyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-1H-indole-2-thiolate

: 917247-59-7
1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.70 g / acetone / 0.5 h / 20 °C

2: 88 percent / Et₃N / acetonitrile / 24 h / 20 °C

With triethylamine; In acetone; acetonitrile;
DOI:10.1080/15257770500265646

Reference yield:

: 174808-03-8
5,6-dichloroindole-2-thione

: 917247-59-7
1-acetyl-3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)-2-benzylthio-5,6-dichloroindole

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂CO₃ / methanol / 20 h / 20 °C

2: 1.70 g / acetone / 0.5 h / 20 °C

3: 88 percent / Et₃N / acetonitrile / 24 h / 20 °C

With sodium carbonate; triethylamine; In methanol; acetone; acetonitrile; 1: Knoevenagel coupling;
DOI:10.1080/15257770500265646