2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

Base Information

Chemical Name:2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride
CAS No.:162635-10-1
Molecular Formula:C₁₅H₁₅Cl₃O₅
Molecular Weight:381.64
Hs Code.:

Synonyms:2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

Suppliers and Price of 2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

There total 2 articles about 2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16837-14-2
2,2,5-trimethyl-1,3-dioxane-5-carboxylic acid

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 162635-10-1
2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 5h;

Reference yield:

: 4767-03-7
2,2-bis(hydroxymethyl)propionic acid

: 162635-10-1
2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

1.2: 3 h

2.1: triethylamine / dichloromethane / 2.5 h / 0 - 25 °C

With triethylamine; toluene-4-sulfonic acid; In dichloromethane; benzene;

Reference yield: 96.3%

: 162635-10-1
2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride

: C₅₅H₈₆F₃NO₁₅SSi

: C₆₂H₉₉NO₁₆Si

Guidance literature:: 2,4,6-trichlorobenzoic-2',2',5'-trimethyl-1',3'-dioxane-5'-carboxylic anhydride; C₅₅H₈₆F₃NO₁₅SSi; In dichloromethane; at -20 ℃; for 0.333333h;

With dmap; In dichloromethane; at -25 ℃; Temperature; Reagent/catalyst;