7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine

Base Information

Chemical Name:7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine
CAS No.:1648787-47-6
Molecular Formula:C₄₈H₃₃NS
Molecular Weight:655.863
Hs Code.:

Synonyms:7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine

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Chemical Property of 7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine

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Technology Process of 7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine

There total 2 articles about 7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 114773-97-6
2-(α-methoxyimino)ethylthiophene

: 501-65-5
diphenyl acetylene

: 1648787-47-6
7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; sodium acetate; In methanol; at 110 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201400292

Reference yield: 61.0%

: 88-15-3,97511-16-5
2-Acetylthiophene

: 501-65-5
diphenyl acetylene

: 1648787-47-6
7-methyl-4-phenyl-5-(5,6,7,8-tetraphenylnaphthalen-1-yl)-thieno[2,3-c]pyridine

Guidance literature:: 2-Acetylthiophene; diphenyl acetylene; With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) acetate; hydroxylamine-O-sulfonic acid; In methanol; at 70 ℃; Schlenk technique; Inert atmosphere;

With copper diacetate; In methanol; at 110 ℃; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.0c02582