4-HYDROXYPHENYLDIMETHYLSULFONIUM METHYL SULFATE

Base Information

• Chemical Name: 4-HYDROXYPHENYLDIMETHYLSULFONIUM METHYL SULFATE
• CAS No.: 32279-04-2
• Molecular Formula: C9H14O5S2
• Molecular Weight: 266.339
• Hs Code.: 2930909090
• Mol file: 32279-04-2.mol

Synonyms:4-HYDROXYPHENYLDIMETHYLSULFONIUM METHYL SULFATE;DIMETHYL-4-HYDROXYPHENYLSULFONIUM METHYL SULFATE

Chemical Property of 4-HYDROXYPHENYLDIMETHYLSULFONIUM METHYL SULFATE

Chemical Property:

• Melting Point: 92 °C
• PSA: 120.34000
• LogP: 1.80280

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-Hydroxyphenyldimethylsulfonium Methyl Sulfate >98.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-HYDROXYPHENYLDIMETHYLSULFONIUM METHYL SULFATE

There total 1 articles about 4-HYDROXYPHENYLDIMETHYLSULFONIUM METHYL SULFATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxythioanisole (1073-72-9) + dimethyl sulfate (77-78-1) → (p-hydroxyphenyl)dimethylsulfonium methyl sulfate (32279-04-2)

Guidance literature:

at 100 ℃;

DOI:10.1021/ja01551a045 DOI:10.1021/ja01582a027

Reference yield: 97.0%

sodium hexafluoroantimonate (16925-25-0) + (p-hydroxyphenyl)dimethylsulfonium methyl sulfate (32279-04-2) → (4-hydroxyphenyl)dimethylsulfonium hexafluoroantimonate

Guidance literature:

In Isopropyl acetate; at 10 ℃; for 0.5h;

Reference yield: 92.0%

Z-Ser(Bzl)-OH (20806-43-3) + (p-hydroxyphenyl)dimethylsulfonium methyl sulfate (32279-04-2) → Z-Ser(Bzl)-DSP

Guidance literature:

With dicyclohexyl-carbodiimide; In acetonitrile; at 0 ℃;

upstream raw materials:

4-hydroxythioanisole

dimethyl sulfate

Downstream raw materials:

Z-Ile-O-kojiate

Refernces