Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

Base Information

Chemical Name:Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester
CAS No.:77262-58-9
Molecular Formula:C₂₅H₂₉ClO₇
Molecular Weight:476.954
Hs Code.:

Synonyms:Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

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Chemical Property of Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

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Technology Process of Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

There total 3 articles about Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 85-44-9
phthalic anhydride

: 67726-66-3
1-<4-<4-(3-Chloro-2-tetrahydrofuryloxy)butoxy>phenyl>propanol

: 77262-58-9
Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

Guidance literature:: With pyridine; at 60 ℃; for 10h;
DOI:10.1021/je00024a041

Reference yield:

: 20191-97-3
2-(4-Chlorobutoxy)-3-chlorotetrahydrofuran

: 77262-58-9
Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / KOH / dimethylformamide / 2 h / 60 - 70 °C

2: LiAlH₄ / diethyl ether / 0.5 h / Heating

3: 55 percent / pyridine / 10 h / 60 °C

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/je00024a041

Reference yield:

: 67726-56-1
4-<4-(3-Chloro-2-tetrahydrofuryloxy)butoxy>propiophenone

: 77262-58-9
Phthalic acid mono-(1-{4-[4-(3-chloro-tetrahydro-furan-2-yloxy)-butoxy]-phenyl}-propyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0.5 h / Heating

2: 55 percent / pyridine / 10 h / 60 °C

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/je00024a041