N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

Base Information

Chemical Name:N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide
CAS No.:1202017-17-1
Molecular Formula:C₂₀H₂₁NO₂S
Molecular Weight:339.458
Hs Code.:

Synonyms:N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

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Technology Process of N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

There total 2 articles about N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 85217-69-2,87802-71-9
cinnamyl methyl carbonate

: 286376-23-6
4-methyl-N-(prop-1-yn-1-yl)benzenesulfonamide

: 1051370-38-7
N-(but-2-ynyl)-N-cinnamyl-4-methylbenzenesulfonamide

: 1202017-17-1
N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; In tetrahydrofuran; at 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201000467

Reference yield: 88.0%

: 85217-69-2,87802-71-9
cinnamyl methyl carbonate

: 286376-23-6
4-methyl-N-(prop-1-yn-1-yl)benzenesulfonamide

: 1202017-17-1
N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

: N-(but-2-yn-1-yl)-4-methyl-N-[(2E)-3-phenylprop-2-en-1-yl]benzenesulfonamide

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; [O,O’-((S)-1,1′-dinaphthyl-2,2′-diyl)-N,N′-di-(S,S)-1-(2-methoxyphenyl)ethylphosphoramidite]; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 20 ℃; for 6h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000706

Reference yield: 52.0%

: 1202017-17-1
N-(but-2-yn-1-yl)-4-methyl-N-[(1S)-1-phenylprop-2-en-1-yl]benzenesulfonamide

: 1239131-26-0
C₂₀H₂₁NO₂S

Guidance literature:: With cis-dichloroplatinum; In tetrahydrofuran; for 24h; optical yield given as %ee; enantioselective reaction; Reflux; Inert atmosphere;
DOI:10.1002/chem.201000467