4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

Base Information

Chemical Name:4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide
CAS No.:1198088-06-0
Molecular Formula:BrH*C₂₄H₂₀N₄O₃S
Molecular Weight:525.426
Hs Code.:

Synonyms:4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

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Chemical Property of 4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

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Technology Process of 4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

There total 6 articles about 4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 2114-02-5
amidinothiocarbamide

: 1198088-05-9
4-(2-bromoacetyl)phenyl 3'-methoxybiphenyl-4-carboxylate

: 1198088-06-0
4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

Guidance literature:: In acetone; Reflux;

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 1198088-06-0
4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 6 h / 80 °C / Inert atmosphere

2: thionyl chloride

3: sodium hydride / dichloromethane; mineral oil

4: bromine; acetic acid

5: acetone / Reflux

With thionyl chloride; bromine; sodium hydride; caesium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water; acetone; mineral oil;

Reference yield:

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 1198088-06-0
4-(2-guanidinothiazol-4-yl)phenyl 3'-methoxybiphenyl-4-carboxylate hydrobromide

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 6 h / 80 °C / Inert atmosphere

2: thionyl chloride

3: sodium hydride / dichloromethane; mineral oil

4: bromine; acetic acid

5: acetone / Reflux

With thionyl chloride; bromine; sodium hydride; caesium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water; acetone; mineral oil;