N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

Base Information

Chemical Name:N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin
CAS No.:145593-78-8
Molecular Formula:C₂₁H₂₃N₃O₇
Molecular Weight:429.43
Hs Code.:

N<sup>4</sup>-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

Synonyms:N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

Suppliers and Price of N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

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Technology Process of N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

There total 1 articles about N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 26661-13-2
4-N-benzoylcytosine

: 23339-17-5
methyl 4,6-di-O-acetyl-2,3-dideoxy-D-erythro-hexopyranoside

: 52945-57-0
4,6-di-O-acetyl-1,5-anhydro-2,3-dideoxy-D-erythro-hex-1-enitol

: 145593-79-9
N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-α-D-glucopyranosyl)cytosin

: 145593-78-8
N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; tin(IV) chloride; In acetonitrile; 1) r.t., 30 min, 2) 45 - 50 deg C, 2 h;
DOI:10.1002/hlca.19920750503

Reference yield: 86.0%

: 145593-78-8
N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

: 145593-86-8
N⁴-Benzoyl-1-(2',3'-dideoxy-β-D-glucopyranosyl)cytosin

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 ℃; for 0.416667h;
DOI:10.1002/hlca.19920750503

Reference yield:

: 145593-78-8
N⁴-Benzoyl-1-(4',6'-di-O-acetyl-2',3'-dideoxy-β-D-glucopyranosyl)cytosin

: 145594-00-9
N⁴-Benzoyl-1-<2',3'-dideoxy-6'-O-<(4,4'-dimethoxytriphenyl)methyl>-β-D-glucopyranosyl>cytosin

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 2N aq. NaOH / tetrahydrofuran; methanol; H₂O / 0.42 h / 0 °C

2: 88 percent / pyridine / (Bu₄N)ClO₄ / 1 h / Ambient temperature

With pyridine; sodium hydroxide; tetrabutylammonium perchlorate; In tetrahydrofuran; methanol; water;
DOI:10.1002/hlca.19920750503