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Technology Process of [(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]

[(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]

Base Information
  • Chemical Name:[(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]
  • CAS No.:317373-65-2
  • Molecular Formula:C22H45O2P2Ru*C24H20B
  • Molecular Weight:823.849
  • Hs Code.:
[(C<sub>5</sub>(CH<sub>3</sub>)5)Ru(O<sub>2</sub>)(P(C<sub>2</sub>H<sub>5</sub>)3)2]<sup>(1+)</sup>*[B(C<sub>6</sub>H<sub>5</sub>)4]<sup>(1-)</sup>=[(C<sub>5</sub>(CH<sub>3</sub>)5)Ru(O<sub>2</sub>)(P(C<sub>2</sub>H<sub>5</sub>)3)2][B(C<sub>6</sub>H<sub>5</sub>)4]

Synonyms:[(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]

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Chemical Property of [(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]
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Technology Process of [(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]

There total 1 articles about [(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Cp(*)(triethylphosphine)2RuCl

Cp(*)(triethylphosphine)2RuCl

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

[(C<sub>5</sub>(CH<sub>3</sub>)5)Ru(O<sub>2</sub>)(P(C<sub>2</sub>H<sub>5</sub>)3)2]<sup>(1+)</sup>*[B(C<sub>6</sub>H<sub>5</sub>)4]<sup>(1-)</sup>=[(C<sub>5</sub>(CH<sub>3</sub>)5)Ru(O<sub>2</sub>)(P(C<sub>2</sub>H<sub>5</sub>)3)2][B(C<sub>6</sub>H<sub>5</sub>)4]
317373-65-2

[(C5(CH3)5)Ru(O2)(P(C2H5)3)2](1+)*[B(C6H5)4](1-)=[(C5(CH3)5)Ru(O2)(P(C2H5)3)2][B(C6H5)4]

Guidance literature:
With air; In methanol; excess of NaBPh4 added to Ru complex soln. under air, stirred for 10-15min; ppt. filtered off, washed (EtOH and petroleum ether), dried (vac.), recrystd. (acetone//EtOH); elem. anal.;
DOI:10.1016/s0022-328x(00)00176-5
upstream raw materials:

sodium tetraphenyl borate

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