cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-N=CH-4-⁽¹⁸⁾F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl

Base Information

• Chemical Name: cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-N=CH-4-⁽¹⁸⁾F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl
• CAS No.: 1361405-56-2
• Molecular Formula: C₅₀H₆₂FN₁₁O₁₁
• Molecular Weight: 1011.11

Synonyms:cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-N=CH-4-⁽¹⁸⁾F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl

Chemical Property of cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-N=CH-4-⁽¹⁸⁾F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl

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Technology Process of cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-N=CH-4-⁽¹⁸⁾F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl

There total 1 articles about cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-N=CH-4-⁽¹⁸⁾F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG2-O-NH2)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl (1361405-54-0) + 4-trimethylammoniumbenzaldehyde triflate → cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG2-O-N=CH-4-NMe2-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl (1361405-55-1) + cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG2-O-N=CH-4-(18)F-Ph)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl (1361405-56-2)

Guidance literature:

4-trimethylammoniumbenzaldehyde triflate; With [¹⁸F]-potassium fluoride; potassium hydrogencarbonate; [2.2.2]cryptande; In dimethyl sulfoxide; at 80 ℃; for 0.00416667h; Inert atmosphere; Microwave irradiation;

cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-NH₂)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl; With ammonium formate; In methanol; at 80 ℃; for 0.333333h; pH=2; chemoselective reaction; aq. buffer;

DOI:10.1016/j.jfluchem.2011.11.003

upstream raw materials:

cyclo-[Nal-Gly-(D-Tyr)-Orn(PEG₂-O-NH₂)-Arg], Nal = 3-(naphthalen-2-yl)alaninoyl

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