4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose

Base Information

• Chemical Name: 4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose
• CAS No.: 1101200-00-3
• Molecular Formula: C₄₆H₅₀O₇Si
• Molecular Weight: 742.984

Synonyms:4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose

Chemical Property of 4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose

Chemical Property:

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Technology Process of 4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose

There total 1 articles about 4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2,6-anhydro-3,4,5-tri-O-benzyl-1-O-(tert-butyldiphenylsilyl)-7,8,9-trideoxy-D-glycero-L-gulo-non-7-ynitol (1101199-97-6) → 4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose (1101200-00-3)

Guidance literature:

With sodium periodate; ruthenium (IV) oxide monohydrate; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 1h; Darkness;

DOI:10.1002/anie.200803696

Reference yield: 65.0%

4,8-anhydro-5,6,7-tri-O-benzyl-9-O-tert-butyldiphenylsilyl-1-deoxy-D-glycero-D-idonono-2,3-diulose (1101200-00-3) → C46H50O7Si (1101200-01-4)

Guidance literature:

In chloroform-d1; at 20 ℃; for 3h; Irradiation;

DOI:10.1002/anie.200803696

upstream raw materials:

2,6-anhydro-3,4,5-tri-O-benzyl-1-O-(tert-butyldiphenylsilyl)-7,8,9-trideoxy-D-glycero-L-gulo-non-7-ynitol

Downstream raw materials:

C₄₆H₅₀O₇Si

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