Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI)
CAS No.:217442-28-9
Molecular Formula:C₉H₁₁NO₃
Molecular Weight:181.191
Hs Code.:
Mol file:217442-28-9.mol

Synonyms:Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI)

Suppliers and Price of Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI)

Chemical Property:

PSA：55.40000
LogP:0.88030

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI)

There total 2 articles about Carbamic acid, [1-(3-oxo-1-propynyl)-3-butenyl]-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 217442-22-3
[1-(3,3-Diethoxy-prop-1-ynyl)-but-3-enyl]-carbamic acid methyl ester

: 217442-28-9
[1-(3-Oxo-prop-1-ynyl)-but-3-enyl]-carbamic acid methyl ester

Guidance literature:: With formic acid; In chloroform; at 40 ℃; for 3h;
DOI:10.1016/S0022-328X(98)00857-2

Reference yield:

: 217442-00-7
7,7-diethoxyhept-1-en-5-yn-4-ylamine

: 217442-28-9
[1-(3-Oxo-prop-1-ynyl)-but-3-enyl]-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Et₃N, K₂CO₃ / CHCl₃ / 12 h / Heating

2: 70 percent / HCOOH / CHCl₃ / 3 h / 40 °C

With formic acid; potassium carbonate; triethylamine; In chloroform;
DOI:10.1016/S0022-328X(98)00857-2