2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone

Base Information

Chemical Name:2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone
CAS No.:874350-76-2
Molecular Formula:C₁₉H₂₇N₃O₅Si
Molecular Weight:405.526
Hs Code.:

Synonyms:2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone

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Chemical Property of 2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone

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Technology Process of 2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone

There total 1 articles about 2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: sodium azide

: 874350-75-1
3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-D-gulonolactone

: 874350-76-2
2-azido-3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-2-deoxy-D-gulonolactone

Guidance literature:: 3,5-O-benzylidene-6-O-tert-butyldimethylsilyl-D-gulonolactone; With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -20 ℃; for 1h;

sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

With pyridinium p-toluenesulfonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;