(η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium

Base Information

Chemical Name:(η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium
CAS No.:173977-48-5
Molecular Formula:C₁₈H₂₆P₂Ti
Molecular Weight:352.232
Hs Code.:

Synonyms:(η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium

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Technology Process of (η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium

There total 2 articles about (η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 12112-27-5,646059-44-1,1252659-06-5
(η4-cyclooctatetraene)(η8-cycloctatetraene)titanium

: 78129-68-7
2,2-dimethylpropylidynephosphine

: 173977-48-5
(η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium

: 164358-72-9,165883-57-8
3,4,7,8-Tetra-tert-butyl-1,2,5,6-tetraphospha-tricyclo[4.2.0.0^2,5]octa-3,7-diene

Guidance literature:: With hexachloroethane; In toluene; pentane; byproducts: TiCl2(C8H8), C2Cl4; (argon); 85°C, 2 d, solvent removal (vac.), dissoln. (pentane), addn. of hexachloroethane, stirring (20°C, 5 d); filtration, cooling to -78°C;

Reference yield:

: 12112-27-5,646059-44-1,1252659-06-5
(η4-cyclooctatetraene)(η8-cycloctatetraene)titanium

: 78129-68-7
2,2-dimethylpropylidynephosphine

: 173977-51-0
(η(8)-cyclooctatetraene)(η(4)-3,4-di-tert-butyl-1,2-diphosphete)titanium

: 173977-48-5
(η(8)-cyclooctatetraene)(η(4)-2,4-di-tert-butyl-1,3-diphosphete)titanium

Guidance literature:: In toluene; (argon); 85°C, 2 d; solvent removal (vac.), dissoln. (pentane), filtration, cooling to -78°C, crystn. after 6 d, filtration, drying (vac.), manual sepn. of crystals of the byproduct;