1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

Base Information

Chemical Name:1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide
CAS No.:84786-82-3
Molecular Formula:C₂₆H₂₈O₃P*I
Molecular Weight:546.385
Hs Code.:

Synonyms:1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

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Chemical Property of 1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

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Technology Process of 1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

There total 6 articles about 1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 84786-97-0
1-(2-iodoethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

: 603-35-0
triphenylphosphine

: 84786-82-3
1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

Guidance literature:: With sodium hydrogencarbonate; In acetonitrile; for 20h; Heating;
DOI:10.1016/S0040-4020(01)86469-3

Reference yield:

: 77-85-0
2-(hydroxymethyl)-2-methylpropane-1,3-diol

: 84786-82-3
1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 3 h / 40 °C

2: NaI / dimethylformamide / 3 h / 100 °C

3: K₂CO₃ / acetonitrile / 24 h / Heating

With potassium carbonate; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00344a047

Reference yield:

: 84786-96-9
1-(2-chloroethyl)-4-methyl-2,6,7-trioxabicyclo[2.2.2]octane

: 84786-82-3
1-(2-triphenylphosphoniumethyl)-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane iodide

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / dimethylformamide / 3 h / 100 °C

2: K₂CO₃ / acetonitrile / 24 h / Heating

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00344a047