cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride

Base Information

Chemical Name:cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride
CAS No.:344414-37-5
Molecular Formula:C₁₆H₉Cl₃O₃
Molecular Weight:355.605
Hs Code.:

Synonyms:cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride

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Technology Process of cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride

There total 2 articles about cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 344414-37-5
cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride

Guidance literature:: With triethylamine; In tetrahydrofuran; for 0.5h;
DOI:10.1021/jo951895e

Reference yield:

: 621-82-9
Cinnamic acid

: 344414-37-5
cinnamoyl 2,4,6-trichlorobenzoyl mixed anhydride

Guidance literature:: Cinnamic acid; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

With 2,4,6-trichlorobenzoyl chloride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.10.016