3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester

Base Information

• Chemical Name: 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester
• CAS No.: 128049-95-6
• Molecular Formula: C₂₁H₂₃NO₈
• Molecular Weight: 417.416

Synonyms:3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester

Chemical Property of 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester

Chemical Property:

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Technology Process of 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester

There total 6 articles about 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzo[1,3]dioxol-5-yl-2-(3,4,5-trimethoxy-benzoylamino)-acrylic acid methyl ester (116603-73-7) → 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester (128049-95-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; under 760 Torr; Yield given;

DOI:10.1016/S0040-4039(01)80681-X

Reference yield:

piperonal (120-57-0,30024-74-9) → 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester (128049-95-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / Ac₂O, NaOAc

2: K₂CO₃ / Ambient temperature

3: H₂ / Pd/C / 760 Torr

With hydrogen; sodium acetate; acetic anhydride; potassium carbonate; palladium on activated charcoal;

DOI:10.1016/S0040-4039(01)80681-X

Reference yield:

(3,4,5-trimethoxybenzoylamino)acetic acid (40915-27-3) → 3,4-methylenedioxy-N-(3,4,5-trimethoxy-benzoyl)-phenylalanine-methyl ester (128049-95-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / Ac₂O, NaOAc

2: K₂CO₃ / Ambient temperature

3: H₂ / Pd/C / 760 Torr

With hydrogen; sodium acetate; acetic anhydride; potassium carbonate; palladium on activated charcoal;

DOI:10.1016/S0040-4039(01)80681-X

upstream raw materials:

3-benzo[1,3]dioxol-5-yl-2-(3,4,5-trimethoxy-benzoylamino)-acrylic acid methyl ester

piperonal

(3,4,5-trimethoxybenzoylamino)acetic acid

4-piperonylidene-2-(3,4,5-trimethoxy-phenyl)-4H-oxazol-5-one

Downstream raw materials:

5-methoxy-4-piperonyl-2-(3,4,5-trimethoxy-phenyl)-oxazole

5-(3,4,5-trimethoxy-phenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinoline-7-carboxylic acid methyl ester

(3aR,10R)-2-Methyl-10-(3,4,5-trimethoxy-phenyl)-3,3a,4,10-tetrahydro-2H-6,8-dioxa-1-thia-2,10a-diaza-dicyclopenta[b,g]naphthalene 1-oxide

(3aS,10S)-10-(3,4,5-Trimethoxy-phenyl)-3,3a,4,10-tetrahydro-2,6,8-trioxa-1-thia-10a-aza-dicyclopenta[b,g]naphthalene 1-oxide

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