Technology Process of C27H37NO2
There total 11 articles about C27H37NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H30O3;
With
dmap; methanesulfonyl chloride; triethylamine;
In
dichloromethane;
at -20 - 20 ℃;
for 0.333333h;
benzylamine;
In
dichloromethane;
for 3h;
Further stages.;
DOI:10.1016/j.tetlet.2007.07.184
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / LAH / tetrahydrofuran / 0 - 20 °C
2: 95 percent / Dess-Martin periodinane / CH2Cl2 / 0 - 20 °C
3: 95 percent / DDQ / CH2Cl2; H2O / 20 °C
4: Et3N; MsCl; DMAP / CH2Cl2 / 2 h / -20 - 40 °C
5: CH2Cl2 / 3 h / 20 °C
With
dmap; lithium aluminium tetrahydride; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; dichloromethane; water;
5: double aza-Michael reaction;
DOI:10.1016/j.tetlet.2007.07.184
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / Dess-Martin periodinane / CH2Cl2 / 0 - 20 °C
2: 95 percent / DDQ / CH2Cl2; H2O / 20 °C
3: Et3N; MsCl; DMAP / CH2Cl2 / 2 h / -20 - 40 °C
4: CH2Cl2 / 3 h / 20 °C
With
dmap; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water;
4: double aza-Michael reaction;
DOI:10.1016/j.tetlet.2007.07.184
