Technology Process of C34H54O6Si
There total 6 articles about C34H54O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; hydrogen; ethylenediamine;
nickel diacetate;
In
ethanol;
at 23 ℃;
for 5h;
under 760.051 Torr;
DOI:10.1016/j.bmcl.2007.01.096
- Guidance literature:
-
Multi-step reaction with 4 steps
1: OsO4; NMO / 2-methyl-propan-2-ol / 12 h / 23 °C
2: NaIO4/SiO2 / CH2Cl2 / 1.5 h / 23 °C
3: NaN(SiMe3)2 / toluene; tetrahydrofuran / -90 - 23 °C
4: 85 percent / NaBH4; (H2NCH2)2; H2 / Ni(OAc)2 / ethanol / 5 h / 23 °C / 760.05 Torr
With
sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; hydrogen; sodium hexamethyldisilazane; silica gel; ethylenediamine;
nickel diacetate;
In
tetrahydrofuran; ethanol; dichloromethane; toluene; tert-butyl alcohol;
3: Wittig olefination;
DOI:10.1016/j.bmcl.2007.01.096
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaIO4/SiO2 / CH2Cl2 / 1.5 h / 23 °C
2: NaN(SiMe3)2 / toluene; tetrahydrofuran / -90 - 23 °C
3: 85 percent / NaBH4; (H2NCH2)2; H2 / Ni(OAc)2 / ethanol / 5 h / 23 °C / 760.05 Torr
With
sodium tetrahydroborate; sodium periodate; hydrogen; sodium hexamethyldisilazane; silica gel; ethylenediamine;
nickel diacetate;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;
2: Wittig olefination;
DOI:10.1016/j.bmcl.2007.01.096
