3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester

Base Information

• Chemical Name: 3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester
• CAS No.: 854819-60-6
• Molecular Formula: C₁₆H₂₆N₄O₄
• Molecular Weight: 338.407

Synonyms:3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester

Chemical Property of 3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of 3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester

There total 2 articles about 3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,5-dimethyl-p-phenylene)-bis-hydrazine-N,N'-dicarboxylic acid tetraethyl ester (6304-69-4) → 3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester (854819-60-6)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

Reference yield:

para-xylene (106-42-3) → 3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester (854819-60-6)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄

2: LiAlH₄; diethyl ether

With lithium aluminium tetrahydride; diethyl ether; sulfuric acid;

Reference yield:

3,3'-dimethyl-3,3'-(2,5-dimethyl-p-phenylene)-bis-carbazic acid diethyl ester (854819-60-6) → N,N'-dimethyl-N,N'-(2,5-dimethyl-p-phenylene)-bis-acetamide (79817-50-8)

Guidance literature:

With phosphorus; hydrogen iodide; acetic acid; anschliessende Reaktion mit Acetanhydrid und Kaliumacetat;

upstream raw materials:

(2,5-dimethyl-p-phenylene)-bis-hydrazine-N,N'-dicarboxylic acid tetraethyl ester

para-xylene

Downstream raw materials:

N,N'-dimethyl-N,N'-(2,5-dimethyl-p-phenylene)-bis-acetamide

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