C₁₈H₂₃NO₃

Base Information

• Chemical Name: C₁₈H₂₃NO₃
• CAS No.: 1418022-82-8
• Molecular Formula: C₁₈H₂₃NO₃
• Molecular Weight: 301.386
• Mol file: 1418022-82-8.mol

Synonyms:C₁₈H₂₃NO₃

Chemical Property of C₁₈H₂₃NO₃

Chemical Property:

Purity/Quality:

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Technology Process of C₁₈H₂₃NO₃

There total 1 articles about C₁₈H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H17NO3 (1399842-84-2) + 1-Bromo-2-butyne (3355-28-0) → C18H23NO3 (1418022-82-8)

Guidance literature:

With indium; ammonium chloride; In tetrahydrofuran; water; at 0 ℃;

DOI:10.1002/adsc.201400928

Reference yield: 58.0%

C18H23NO3 (1418022-82-8) + acetic anhydride (108-24-7) → C20H25NO4 (1418022-69-1)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c2cc37872h

Reference yield: 45.0%

C18H23NO3 (1418022-82-8) + dimethyl sulfate (77-78-1) → C19H25NO3 (1418022-70-4)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydroxide; In dichloromethane; water; at 20 ℃;

DOI:10.1039/c2cc37872h

upstream raw materials:

C₁₄H₁₇NO₃

1-Bromo-2-butyne

Downstream raw materials:

C₂₀H₂₅NO₄

C₁₉H₂₅NO₃