(S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

Base Information

Chemical Name:(S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester
CAS No.:59903-67-2
Molecular Formula:C₁₆H₂₃NO₂
Molecular Weight:261.364
Hs Code.:

Synonyms:(S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

Suppliers and Price of (S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

There total 1 articles about (S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17431-03-7
L-valine ethyl ester

: 103-79-7,136675-26-8
1-phenyl-acetone

: 59903-67-2
(S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

Guidance literature:: In benzene; for 48h; Heating;
DOI:10.1248/cpb.31.887

Reference yield:

: 59903-67-2
(S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

: 20201-24-5
ethyl 3-methyl-2-oxobutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature

2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C

3: sodium ethoxide / ethanol / 1 h / 40 °C

4: 5percent sulfuric acid / H₂O / 2 h / Ambient temperature

With tert-butylhypochlorite; sulfuric acid; hydrogen; sodium ethanolate; palladium on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1248/cpb.31.887

Reference yield:

: 59903-67-2
(S)-3-Methyl-2-[1-methyl-2-phenyl-eth-(Z)-ylideneamino]-butyric acid ethyl ester

: 51-64-9,17108-96-2,96332-84-2
dexamfetamine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature

2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C

3: sodium ethoxide / ethanol / 1 h / 40 °C

4: 5percent sulfuric acid / H₂O / 2 h / Ambient temperature

With tert-butylhypochlorite; sulfuric acid; hydrogen; sodium ethanolate; palladium on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1248/cpb.31.887