tert-butyl allyl(phenyl)carbamate

Base Information

Chemical Name:tert-butyl allyl(phenyl)carbamate
CAS No.:169268-95-5
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:tert-butyl allyl(phenyl)carbamate

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Chemical Property of tert-butyl allyl(phenyl)carbamate

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Technology Process of tert-butyl allyl(phenyl)carbamate

There total 6 articles about tert-butyl allyl(phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 589-09-3
N-allyl-N-phenylamine

: 24424-99-5
di-tert-butyl dicarbonate

: 169268-95-5
tert-butyl allyl(phenyl)carbamate

Guidance literature:: With triethylamine; at 130 ℃; for 2h;
DOI:10.1080/00397919508015894

Reference yield: 94.0%

: 3422-01-3
tert-butyl phenylcarbamate

: 106-95-6
allyl bromide

: 169268-95-5
tert-butyl allyl(phenyl)carbamate

Guidance literature:: tert-butyl phenylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1.5h; Inert atmosphere;

allyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol5018257

Reference yield: 91.0%

: 1345987-89-4
C₁₄H₁₇NO₂

: 169268-95-5
tert-butyl allyl(phenyl)carbamate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; formic acid; XPhos; In tetrahydrofuran; 1,2-dichloro-ethane; at 40 ℃; for 12h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.202103402